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SPTS CPX Clutser for dieletric etching and metal etching and PECVD of SiO2, SiNx and a-Si.
Also, Plasma Asher, CVD hot wall tube furnace for graphene and CNTs growth
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Comprehensive set of metrology systems to monitor process output and characterize devices: optical and contact profilometry, optical inspection, Sheet Resistance measurement, Wafer prober, wire bonders
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The Prototyping lab is used for electronics assembly and fabrication of accessories/parts to support device packaging and experimental testing mountings.
The most used tool is the Laser Engraving and Cutting tool that uses using computer numerical control to cut several compatible plastic materials such as PE, PP, PETG, PA, PMMA, etc. It is used for very diverse purposes by several groups such as microfluidic platforms. The 3D printers (extruder for 1.75mm diameter filaments; nozzle size 400µm) are frequently used for prototyping and building experimental assembly accessories. The stereolithography 3D Printer SLA Formlabs Form2 which uses laser to cure solid parts from liquid resins (minimum feature size 150 µm; layer resolution 25-100 µm) is also used for microneedle molds fabrication.
This lab features also a soldering station (JBC DDE) with precision soldering tips, desoldering unit and hot air for small volume prototyping and rework.
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The MEMS lab is focused on the (electrical, mechanical, optical) characterization of MEMS i.e. microelectromechanical systems as well as other types of devices and transducers fabricated in our cleanroom.
It comprises a large diversity of electronic instrumentation such as LCR meters, power supplies, function generators, lock-in amplifiers, sourcemeters and multimeters.
The electromechanical characterization is also accomplished using characterization instruments that rely also on optical principles such as microsystem analyser Polytec MSA-500, or Polytec UHF-120.
Polytec MSA-500 is an optical measurement tool for MEMS displacement and topography. Three types of measurements can be performed:
1- Static characterization of the topography by scanning white-light interferometry, appropriate for rough and smooth surfaces with sub-nanometer vertical resolution and a horizontal resolution in the sub-micrometer range;
2- Real-time dynamic characterization of out-of-plane vibrations by laser-Doppler vibrometry at frequencies up to 24 MHz with a displacement resolution in the picometer range; and
3- Dynamic characterization of in-plane movements by stroboscopic video microscopy up to 1 MHz with a displacement resolution in the nanometer range. An installed Helmholtz coils setup allows to perform measurements in a wide range of magnetic field conditions.
On the same optical table we have the NanoSurf Flex AFM which is a compact and versatile atomic force microscope. It allows for topographical and metrological imaging of mechanical and magnetic properties of samples in air or liquid.
The Optotherm thermal imaging microscope measures and displays the temperature distribution over the surface of small devices with 5µm/pixel spatial resolution. This enables quick detection of hot spots and thermal gradients and can be used to characterize thermal actuators and transducers.
Polytec’s UHF-120 is a Laser-Doppler Vibrometer (heterodyne interferometer) to characterize MEMS out-of-plane vibrations at ultra high frequencies (frequency bandwidth up to 1.2 GHz). It can be used for RF MEMS, BAW/SAW filters and NEMS.
We have also a climatic test chamber (Weiss WKL 34/70) with a temperature range between -70°C and 180°C with heating and cooling rates of 4°C/min and 3°C/min respectively.
The devices fabricated in the cleanroom can also be characterized and mapped in an automated way at wafer-scale (simultaneous optical inspection and electrical characterization) on motorized 200mm wafer probe stations with the aid of incorporated microscopes and probe needles connected to several equipment controlled by a dedicated software application and also eqquiped with a Faraday enclosure.
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The Applied Nano-Optics Laboratory is home to two advanced polarization based characterization tools based on ellipsometry. Both systems complement each other whereby one delivers fast characterization over large (cm^2) heterogenous areas of thin films, while the other one performs slow but spatially highly resolved measurements (100um^2 Field-Of-View with ~1um resolution). Central to the laboratory is an optical table where currently a Structured Illumination Microscopy set-up is under development in order to assemble an add-on module for Super Resolution (SR) fluorescence microscopy. On the right hand side is located a chemistry workbench with a lipid extrusion workstation. Finally on the left hand side of the laboratory one can find several analytical chemistry set-ups for quantitative gas sensing. At INL several group utilize this facility for gas sensor characterization.
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The Laboratory for Nanostructured Solar Cells is equipped with equipment for the fabrication of thin-film solar cells. The STAR system (SpuTering for Advanced Research) is composed of three interconnected vacuum chambers, each one dedicated to one or several layers of the typical Cu(In,Ga)Se2) thin-film solar cell stack. The molybdenum back contact is deposited in the center chamber, from where the substrate can be transferred to the CIGS chamber, where Cu, In, and Ga are sputtered and Se is evaporated. Finally, transparent conductive oxide layers wof the front contact are deposited in the third chamber.
A second equipment in the lab is a tube furnace /chemical vapor deposition reactor, where samples 2D materials are deposited and Cu(In,Ga)Se2 can be reacted.
Finally, in a third equipment, sulfur-based solar cell materials can be deposited by co-evaporation.
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The Prototyping lab is used for electronics assembly and fabrication of accessories/parts to support device packaging and experimental testing mountings.
The most used tool is the Laser Engraving and Cutting tool that uses using computer numerical control to cut several compatible plastic materials such as PE, PP, PETG, PA, PMMA, etc. It is used for very diverse purposes by several groups such as microfluidic platforms. The 3D printers (extruder for 1.75mm diameter filaments; nozzle size 400µm) are frequently used for prototyping and building experimental assembly accessories. The stereolithography 3D Printer SLA Formlabs Form2 which uses laser to cure solid parts from liquid resins (minimum feature size 150 µm; layer resolution 25-100 µm) is also used for microneedle molds fabrication.
This lab features also a soldering station (JBC DDE) with precision soldering tips, desoldering unit and hot air for small volume prototyping and rework.
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The Laboratory for Nanostructured Solar Cells is equipped with equipment for the fabrication of thin-film solar cells. The STAR system (SpuTering for Advanced Research) is composed of three interconnected vacuum chambers, each one dedicated to one or several layers of the typical Cu(In,Ga)Se2) thin-film solar cell stack. The molybdenum back contact is deposited in the center chamber, from where the substrate can be transferred to the CIGS chamber, where Cu, In, and Ga are sputtered and Se is evaporated. Finally, transparent conductive oxide layers wof the front contact are deposited in the third chamber.
A second equipment in the lab is a tube furnace /chemical vapor deposition reactor, where samples 2D materials are deposited and Cu(In,Ga)Se2 can be reacted.
Finally, in a third equipment, sulfur-based solar cell materials can be deposited by co-evaporation.
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In order to implement the INL 2030 Strategic Vision and our global Mission of “Exploring Interfaces”, the research groups at INL are organised into six main clusters: Clean Energy, Foodture, Precise Personalised Healthtech, Smart Digital NanoSystems, Sustainable Environment and Advanced Materials and Computing.
These clusters focus on identified societal challenges, in order to support an ecosystem of research, technology, and innovation; to target interdisciplinary nanotechnology applications.
https://inl.int/clusters/
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Because microfluidic technologies are so transversal to many of the activities at INL, the microfluidics laboratory is one of the most sought and in highest demand. Here we develop microfluidic devices for: the isolation of rare cells from body fluids; for controlled assembly of lipid- and polymer-based gene delivery formulations; high throughput cell encapsulation and analysis in microdroplets; biomimetic organ-on-a-chip systems; and optical and magnetoresistive lab-on-a-chip systems for analysis of biomarkers in diseases and foodborne pathogens.
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In the ultrafast bio- and nanophotonics (UBNP) lab we use light as an enabling technology for advanced microscopy, spectroscopy, optical characterization and fabrication. Time correlated single photon counting fluorescence lifetime microscopy (TCSPC-FLIM), multi-photon and near-field super resolution microscopy and ODMR (Optically detected magnetic resonance) are possible on 3 advanced custom built microscope setups, with incubator solutions for live cell imaging. 3D structures for cell interaction studies and micro-size optical components can be fabricated via two-photon polymerization (TPP). The lab also includes dedicated anisotropy and exc./emission flurometer and streak camera units for spectrally resolved fluorescence lifetime and energy transfer measurements, as well as high speed equipment for electrical and optical characterization of micro-sized components.
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The XRD/MRD Diffraction Tool from Malvern-Panalytical: With this system we can characterize materials based on their crystallinity, phase reflections, composition, film thickness, interface or surface roughness, and index of refraction. Samples measured can be powders or thin films. This instrument is also capable of measuring diffraction from planes that are perpendicular to the sample's surface, giving us a full picture of thin films in the reciprocal space.
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The Micro and Nanofabrication Facility operates in a 1000 m^2 controlled class 100 and 1000 Cleanroom. This open-access user facility provides support throughout all the development chain in cleanroom processes: device modelling and design, process integration and device fabrication, packaging and testing.
The unique combination of tools and expertise for deposition, patterning, and etching of a broad range of materials enable extensive in-house capabilities for producing electronic, magnetic, optical, or MEMS devices as well as various “hybrid” combinations, e.g., MEMS structures functionalized with magnetic sensors or optomechanical MEMS devices. Additional heterogeneous integration capabilities include structures that combine bottom-up and top-down methods for (self) organization and patterning of nanomaterials and nanostructures.
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In the ultrafast bio- and nanophotonics (UBNP) lab we use light as an enabling technology for advanced microscopy, spectroscopy, optical characterization and fabrication. Time correlated single photon counting fluorescence lifetime microscopy (TCSPC-FLIM), multi-photon and near-field super resolution microscopy and ODMR (Optically detected magnetic resonance) are possible on 3 advanced custom built microscope setups, with incubator solutions for live cell imaging. 3D structures for cell interaction studies and micro-size optical components can be fabricated via two-photon polymerization (TPP). The lab also includes dedicated anisotropy and exc./emission flurometer and streak camera units for spectrally resolved fluorescence lifetime and energy transfer measurements, as well as high speed equipment for electrical and optical characterization of micro-sized components.
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A multipurpose electron microscope that is well suited to characterize materials and biological samples. A highlight of the JEM 2100 is its fastreadout “OneView” 4k x 4k CCD camera that operates at 25 fps (300 fps with 512 x 512 pixel). SerialEM is installed on the machine and is used for lowdose imaging, tomogram acquisition and semiautomation.
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A functional biomedical characterization of magnetic nanomaterials and nanoformulations is performed in this lab, where the effect of an applied magnetic field is explored for different applications within the Health arena, alone or in combination, such as magnetic resonance imaging, magnetic hyperthermia or controlled drug delivery. Existing equipment includes a Bruker 1.5T relaxometer for contrast agents analyser, a MR Solutions pre-clinical 3T-MRI scanner for imaging acquisition and several magnetic hyperthermia devices that cover from fundamental calorimetric characterizations to in vitro and in vivo functional validations.
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InnovaLab is purpose-designed and equipped to successfully conduct innovation projects with the industry. Specialized equipment/methodologies/techniques address company-oriented coatings research in the areas of plastic, ceramic, glass, wood, textile, and alloys.
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ChemLab is dedicated for air- and moisture sensitive organic synthesis, preparation and testing of covalent organic frameworks and advanced adsorbent materials and is equipped with two specialized fume hoods for materials synthesis, rotary evaporator, and a microemulsion system.
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Econanolab is the laboratory where the aquatic model organisms used in nanotoxicology tests reside. Freshwater organisms such as zebrafish or cyanobacteria and seawater organisms such as microalgae, Artemia sp. or marine mussels helps us here to understand the toxicity of nanomaterials to make them safer from the design phase.
Inside you will find aquaria, water tanks, filtration systems etc and an incubation chamber with controlled illumination. Basic water quality sensors such as a multiparametric probe (conductivity, dissolved oxygen, temperature, pH), refractometer or specialized kits for measuring other chemical parameters such as ions are day-to-day used here.
Additionally, we count with a modular Raman spectrophotometer Bwtek with a 785 nm laser source for the measurement of water contaminants and an inverted optical microscope Nikon TS2 with colour camera for our observations on the aquatic organisms.
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Because microfluidic technologies are so transversal to many of the activities at INL, the microfluidics laboratory is one of the most sought and in highest demand. Here we develop microfluidic devices for: the isolation of rare cells from body fluids; for controlled assembly of lipid- and polymer-based gene delivery formulations; high throughput cell encapsulation and analysis in microdroplets; biomimetic organ-on-a-chip systems; and optical and magnetoresistive lab-on-a-chip systems for analysis of biomarkers in diseases and foodborne pathogens.
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This is the first established central laboratory for research related to biochemistry. Many different types of experiments are carried out here. Some examples are: studies on new adsorbents for water contaminants, synthesis and functionalization of surfaces or nanomaterials, tissue or cell sample preparation for electron microscopy, biological samples digestions or protein separation.
A cold room with high storage capability set at 4°C allows to perform full experiments on its bench, and hosts the cryogenic container where the main stock of cell lines is stored.
This laboratory counts with an automated sample processor for electron microscopy samples, a gel electrophoresis with transference block for protein separation and identification, as well as the most common appliances such as balance, precision balance, pHmeter, water bath, ultrasounds bath, shakers or centrifuges.
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The sample preparation room for the high accuracy laboratories house a cryo microtome, Vitrobot for cryo sample preparation, a plasma cleaner, vacuum oven, PIPS II precision ion polishing system, and a fume hood for preparing samples for the microscopes.
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The INL Nanophotonics & Bioimaging (NBI) open access user facility for addvanced Live cell and Microscopy features cutting-edge optical instrumentation and the know-how required for characterization of material and life sciences samples. The facility includes commercial super resolution microscope solutions such as Total internal reflection fluorescence (TIRF), direct stochastic optical reconstruction microscopy (dSTORM). Other commercial solutions include, multi laser line confocal microscopy, as well as Phase holotomographic microscope, flow cytometer/ cell sorter. The open access user facility provides support in training, service measurements on cytometry and imaging equipment’s, as well as complementary services, such as specimen/sample preparation or image analysis.
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In this laboratory we characterise nanoscale devices in terms of their electrical perfomance for applications including magnetic sensing, wireless communications and novel computing paradigms. The devices are measured in both a statistical (rapid analysis of thousands of devices) and individual approach in order to optimise the nanofabrication process and to explore the response of the devices to external parameters such as magnetic and electrical fields, temperature, radio frequency signals etc.
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A probe and image corrected (scanning) transmission electron microscope optimized for elemental analysis and high resolution TEM/STEM imaging. The microscope is equipped with a monochromator, four energy dispersive X-ray spectroscopy detectors and a GIF for electron energy loss spectroscopy (Dual EELS). The microscope also has a bi-prism for electron holography. An in-situ sample holder allows heating and biasing experiments.
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The SAXSess Kratky camera: an ideal tool to determine the sizes and shapes of nanostructures with some degree of periodicity (e.g. liquid crystalline phases, covalent organic frameworks, etc). In this particular case, the instrument configuration allows probing both the small-angle (SAXS) and wide-angle (WAXS) regimes, and the periodicities (e.g. distances) that can be probed are in the range of ca. 0.23 to 25 nm, depending on the sample. The samples can be liquid or solid in nature.
The nanoscale information about the arrangements of materials provided by SAXS is an ensemble average over the x-ray illuminated area, and is therefore an excellent complement to direct imaging methods (e.g. TEM, AFM) that have to scan through large sample areas to have representative statistics about the sample.
The SAXS instrument is an Anton Paar SAXSess equipped with image plate detection. The q-range available in the SAXS-WAXS combined configuration is 0.23 to 28.3 nm-1. The system uses a sealed X-ray tube and a Kratky camera (i.e. line collimation) to maximize intensity and allow the detection of more weakly scattering systems, at the expense that in this geometry the systems must be isotropic in nature (i.e. not oriented). Currently we are able to measure a variety of sample types including colloidal dispersions, liquid crystals, and finely ground powders over a range of temperature of ca. 22-80 °C.
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Titan ChemiSTEM is a probe corrected (scanning) transmission electron microscope optimized for elemental analysis and high resolution imaging. The microscope is equipped with four energy dispersive X-ray spectroscopy detectors and a GIF for electron energy loss spectroscopy and energy filtered TEM. The microscope also has a wide pole piece gap and can tilt to ± 70 degrees, making it suitable for tomography.
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Helios 450S is a highly versatile tool that combines SEM with a focused ion beam (FIB) of gallium ions. The SEM operates with a field emission gun (FEG) that provides high beam intensity and stability. Imaging can be done with secondary (for SEM and FIB) and backscattered (for SEM) electrons. A STEM detector delivers resolution of 0.8 nm at 30 kV. For element analysis and mapping an EDX detector is available. An ultra high resolution (UHR) stage and flip stages are available inside the microscope. The machine is used for Lamella preparation for TEM, Cross-section imaging, 3D tomography via “Slice and view” application mode.
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The MEMS lab is focused on the (electrical, mechanical, optical) characterization of MEMS i.e. microelectromechanical systems as well as other types of devices and transducers fabricated in our cleanroom.
It comprises a large diversity of electronic instrumentation such as LCR meters, power supplies, function generators, lock-in amplifiers, sourcemeters and multimeters.
The electromechanical characterization is also accomplished using characterization instruments that rely also on optical principles such as microsystem analyser Polytec MSA-500, or Polytec UHF-120.
Polytec MSA-500 is an optical measurement tool for MEMS displacement and topography. Three types of measurements can be performed:
1- Static characterization of the topography by scanning white-light interferometry, appropriate for rough and smooth surfaces with sub-nanometer vertical resolution and a horizontal resolution in the sub-micrometer range;
2- Real-time dynamic characterization of out-of-plane vibrations by laser-Doppler vibrometry at frequencies up to 24 MHz with a displacement resolution in the picometer range; and
3- Dynamic characterization of in-plane movements by stroboscopic video microscopy up to 1 MHz with a displacement resolution in the nanometer range. An installed Helmholtz coils setup allows to perform measurements in a wide range of magnetic field conditions.
On the same optical table we have the NanoSurf Flex AFM which is a compact and versatile atomic force microscope. It allows for topographical and metrological imaging of mechanical and magnetic properties of samples in air or liquid.
The Optotherm thermal imaging microscope measures and displays the temperature distribution over the surface of small devices with 5µm/pixel spatial resolution. This enables quick detection of hot spots and thermal gradients and can be used to characterize thermal actuators and transducers.
Polytec’s UHF-120 is a Laser-Doppler Vibrometer (heterodyne interferometer) to characterize MEMS out-of-plane vibrations at ultra high frequencies (frequency bandwidth up to 1.2 GHz). It can be used for RF MEMS, BAW/SAW filters and NEMS.
We have also a climatic test chamber (Weiss WKL 34/70) with a temperature range between -70°C and 180°C with heating and cooling rates of 4°C/min and 3°C/min respectively.
The devices fabricated in the cleanroom can also be characterized and mapped in an automated way at wafer-scale (simultaneous optical inspection and electrical characterization) on motorized 200mm wafer probe stations with the aid of incorporated microscopes and probe needles connected to several equipment controlled by a dedicated software application and also eqquiped with a Faraday enclosure.
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Titan ChemiSTEM is a probe corrected (scanning) transmission electron microscope optimized for elemental analysis and high resolution imaging. The microscope is equipped with four energy dispersive X-ray spectroscopy detectors and a GIF for electron energy loss spectroscopy and energy filtered TEM. The microscope also has a wide pole piece gap and can tilt to ± 70 degrees, making it suitable for tomography.
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A probe and image corrected (scanning) transmission electron microscope optimized for elemental analysis and high resolution TEM/STEM imaging. The microscope is equipped with a monochromator, four energy dispersive X-ray spectroscopy detectors and a GIF for electron energy loss spectroscopy (Dual EELS). The microscope also has a bi-prism for electron holography. An in-situ sample holder allows heating and biasing experiments.
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The INL Social Building is comprised of a Guest House with 20 bedrooms, a Nursery for the children of INL personnel, and a polyvalent room that can be used as a gym. This space is the concrete expression of the social principles that INL has since its earliest days, welcoming and supporting its employees and visiting researchers.
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The Bruker Icon Atomic Force Microscope (AFM) incorporates the latest evolution on nanoscale imaging with characterization technologies on a large sample tip-scanning AFM platform. The Icon’s temperature-compensating position sensors render noise levels in the sub-angstroms range for the Z-axis, and angstroms in X-Y. Possible applications for this AFM are: material mapping, electrical characterisation, nanomanipulation and many others.
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Here we house the ESCALAB 250Xi, an ultra-high vacuum (UHV) system to analyze the chemical composition of samples by means of X-ray Photoelectron Spectroscopy (XPS). It has a depth resolution of 1-10 nm via depth profiling, and lateral resolution down to ~1 μm. The complementary techniques that are also available are reflection electron energy loss spectroscopy (REELS), ion scattering spectroscopy (ISS) and ultra violet photoelectron spectroscopy (UPS). The techniques are used to assess the elemental composition and chemical state of the constituent elements for wide range of materials, including thin films, powders, nanoparticles, bio-interfaces, etc.
On the table we have a Fourier transformed infrared spectroscopy (FTIR) system Vertex 80v, a spectrometer to work in the mid-infrared (400-8000 cm-1) and far-infrared/terahertz (down to 5 cm-1) ranges. The spectrometer features accessories to operate in the ATR, transmission and reflection modes, vacuum sample compartment as well as liquid cells. The spectrometer is used for characterization of thin films and monolayers, polymers, inorganic materials, coatings, liquids, etc.
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The INL Cafeteria is much more than just a place where INLers have their meals or a coffee. This is also a space used to discuss projects, check what’s new on the corkboard, or just meet a colleague.
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The unique microscopy platform combines a Nanowizard 3 (JPK, Bruker) Atomic Force Microscope (AFM) with an Aurox Laser Free Spinning Disk Confocal, also known as Differential Spinning Disk (DSD). With this combined setup is possible to acquire simultaneous data from fluorescence and atomic force microscopy data without suffering time-dependent cantilever disruption and heating. This platform is fully dedicated to life sciences research allowing nanomechanical mapping and many others.
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Here, we grow and characterize novel semiconducting two-dimensional materials. Our method enables wafer-scale growth of 2D materials, which are further fabricated to devices in our cleanroom. Furthermore, we investigate materials for photovoltaics, i.e. the conversion of sunlight into electricity. Understanding nanoscale phenomena in thin-film photovoltaic technology based on chalcogenide materials will ultimately enable further improvements in their power conversion efficiencies.
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The INL Auditorium is a versatile space, suitable for hosting a wide variety of events, from conferences, seminars, talks, and colloquiums to meetings. With seating for 200 people, this auditorium is one of the most relevant spaces at INL, symbolizing the place where people meet, discuss and promote the interdisciplinary thinking that is a trademark of INL.
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On the left we can see a system for the growth of 2D materials, individual elements are evaporated onto a heated substrate in an ultra-high vacuum environment, thereby ensuring ultra-pure materials. On the right is a scanning probe microscope, for the advanced nanoscale characterization of 2D and energy materials.
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Because microfluidic technologies are so transversal to many of the activities at INL, the microfluidics laboratory is one of the most sought and in highest demand. Here we develop microfluidic devices for: the isolation of rare cells from body fluids; for controlled assembly of lipid- and polymer-based gene delivery formulations; high throughput cell encapsulation and analysis in microdroplets; biomimetic organ-on-a-chip systems; and optical and magnetoresistive lab-on-a-chip systems for analysis of biomarkers in diseases and foodborne pathogens.
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In this lab, we grow high-quality and large-scale low-dimensional materials for versatile functional applications using chemical vapor deposition method. you can see a couple of chemical vapor deposition systems in this room. In addition, you can also see a few two-temperature zone furnaces for chemical vapor transport growth of low-dimensional single crystals. There are also facilities for preparation of precursors for material growth.
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In the Cell Culture Laboratory, human and animal cell lines are grown in a controlled environment and aseptic conditions. Cell culture is an essential tool in multiple areas of research (health, food, pharmaceutics, cosmetics, etc.) to study basic cell biology, developmental science, or the interaction of drugs or other samples with eukaryotic cells. Different experiments are performed according to the needs of each research group. The aim is often to test samples to predict biological interactions and responses through the evaluation of cell viability, proliferation, migration and invasion, adhesion, apoptosis, oxidative stress, inflammation, among others.
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In the microbiology laboratory we work with many different microorganisms, bacteria, yeast, viruses, etc. We do basic work such as culture and isolation of the microorganisms to be used for different kinds of studies, and we also work in the development of different types of methodologies for the detection and charaterization of the microorganisms or interest. We work in the optimization of the different steps needed to detect a pathogen in food microbiology, the development of novel assays using bacteriphages either for the direct detection of a given pathogen or as a tool to capture them in order to be detected by different techniques.
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Welcome to Natural and Artificial Photonic Structures and Devices lab! Here we perform fabrication and advanced optical characterization of photonic nanostructures. This laboratory is equipped to prepare and cultivate bioinspired optical nanostructures for cost-effective production of living photonic materials. Other materials and nanostructures prepared using microfabrication techniques are also inspected here. Here we also develop novel micro-scatterometry and photoluminescence techniques to determine light-matter interactions at the nanoscale and even in-vivo.
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This shale monolith was formed about 500 million years ago and is far from being an ordinary piece of stone. It was brought from a place that connects Spain and Portugal to serve as INL’s first stone, back in 2008, and it symbolizes the union between both Iberian countries around an ambitious joint scientific project. From this pioneering idea, initiated in 2005, born INL, a “cathedral of science”, made to last for centuries.
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This lab has a vibrating sample magnetometer (VSM) and a superconducting quantum interference device (SQUID) to characterize the magnetic properties of samples. Both equipments measure the magnetization and we can control three parameters: magnetic field, time or temperature. The SQUID is more adequate for low temperature, down to 1.8K, and very high fields, up to 7T, and can measure AC and DC. The VSM for high temperatures, up to 900K with a maximum field of 2.2T. The VSM is also capable to masure transport for current-in-plane devices and magnetic torque.
In this laboratory we also perform magnetic treatment in an oven for 10 wafers, (either 6" or 8" in diameter). We can anneal the wafers up to 400ºC with an applied field of 2T both in plane or perpendicular, giving us the possibility to control the magnetic anisotropy of the samples.
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Welcome to the Food Processing and Nutrition Laboratory. In this laboratory, we conduct research in two main areas: sustainable food packaging and personalised nutrition. The laboratory includes:
(i) equipment for electrospraying, prilling-by-vibration, and nano-spray drying for the encapsulation of micronutrients and active ingredients,
(ii) electrospinning and ultrasonic spray coaters to produce high-performance biodegradable food packaging materials (including active packaging), and
(iii) 3D Food printers for ultimate customisation of nutritional properties, taste, and texture.
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In the molecular biology laboratory we mainly work in the development of nucleic acid-based methods. We have two dinstinct areas, one for sample manipulation and nucleic acid extraction, and a second for sample analysis for what we have different types of equipment including PCR and real-time PCR thermocyclers, BioAnalyzer and GelDoc, among others. In this laboratory we work in the development of novel methodologies with different types of applications, namely in the food industry to avoid food fraud, detect pathogenic microorganisms and assure authenticity, but we also develop assays with clinical interest such as detection of the novel coronavirus. In addition to this, we also develop different kinds of prototypes intended for poin of care testing.
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Is a laboratory with a biosafety level 2 (BSL-2) dedicated to the proper handling of clinical specimens. Here, clinical validations are carried out to test the sensitivity, reliability, and robustness of biosensors and lab-on-a-chip devices for clinical diagnostics. Stroke, sepsis, prostate cancer, or nosocomial infections are some of the complex diseases explored at this laboratory.
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InnovaLab is purpose-designed and equipped to successfully conduct innovation projects with the industry. Specialized equipment/methodologies/techniques address company-oriented coatings research in the areas of plastic, ceramic, glass, wood, textile, and alloys.
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In this lab we study devices made of graphene and other bidimensional materials, such as light detectors, small emitters of light, or chemical sensors. Some of these chemical sensors can be used to detect diseases. The optical devices tested here allow to concentrate light of different colors on the devices and measure the electric signals.
Here we use Raman spectroscopy which is a technique that uses a laser to measure the vibrations of atoms and molecules, and can identify every chemical product. It is very used in nanotechnology when disovering new materials.
The microscope you can see here is used for bidimensional materials. It is equipped with a moving arm. It allows to position microscopic particles one on top of the others and create new materials and devices.
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In the ultrafast bio- and nanophotonics (UBNP) lab we use light as an enabling technology for advanced microscopy, spectroscopy, optical characterization and fabrication. Time correlated single photon counting fluorescence lifetime microscopy (TCSPC-FLIM), multi-photon and near-field super resolution microscopy and ODMR (Optically detected magnetic resonance) are possible on 3 advanced custom built microscope setups, with incubator solutions for live cell imaging. 3D structures for cell interaction studies and micro-size optical components can be fabricated via two-photon polymerization (TPP). The lab also includes dedicated anisotropy and exc./emission flurometer and streak camera units for spectrally resolved fluorescence lifetime and energy transfer measurements, as well as high speed equipment for electrical and optical characterization of micro-sized components.
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In the molecular biology laboratory we mainly work in the development of nucleic acid-based methods. We have two dinstinct areas, one for sample manipulation and nucleic acid extraction, and a second for sample analysis for what we have different types of equipment including PCR and real-time PCR thermocyclers, BioAnalyzer and GelDoc, among others. In this laboratory we work in the development of novel methodologies with different types of applications, namely in the food industry to avoid food fraud, detect pathogenic microorganisms and assure authenticity, but we also develop assays with clinical interest such as detection of the novel coronavirus. In addition to this, we also develop different kinds of prototypes intended for poin of care testing.
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In the Nanobiosensors lab, novel (bio)sensors for environmental monitoring and food safety and control are developed, assembled and tested. These biosensors are able to detect several (bio)chemical substances such as bacteria, toxins, proteins and organic contaminants that are indicators of water contamination, food spoilage and adulteration, and diseases. Such analytical devices are composed by a sensitive biological or biomimetic element (like antibodies, enzymes, nucleic acids, polymers or cell receptors) that interacts and recognizes the analyte, and by a physical transducer (electrochemical, optical, piezoelectric or magnetic), which converts the (bio)chemical signal into a physical quantity that can be measure. These valuable analytical tools allow the fast screening of pathogens, contaminants and disease biomarkers in real-time, at an effective cost and the presentation of the results in a user-friendly way. These sensing devices are usually custom-designed and fabricated to fit the specific applications.
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This lab has a vibrating sample magnetometer (VSM) and a superconducting quantum interference device (SQUID) to characterize the magnetic properties of samples. Both equipments measure the magnetization and we can control three parameters: magnetic field, time or temperature. The SQUID is more adequate for low temperature, down to 1.8K, and very high fields, up to 7T, and can measure AC and DC. The VSM for high temperatures, up to 900K with a maximum field of 2.2T. The VSM is also capable to masure transport for current-in-plane devices and magnetic torque.
In this laboratory we also perform magnetic treatment in an oven for 10 wafers, (either 6" or 8" in diameter). We can anneal the wafers up to 400ºC with an applied field of 2T both in plane or perpendicular, giving us the possibility to control the magnetic anisotropy of the samples.
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ChemLab is dedicated for air- and moisture sensitive organic synthesis, preparation and testing of covalent organic frameworks and advanced adsorbent materials and is equipped with two specialized fume hoods for materials synthesis, rotary evaporator, and a microemulsion system.
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Welcome to Nanofabrication for Optoelectronic Applications (NOA) Laboratory! In here, we conduct advanced thermal and electrical characterization of optoelectronic and energy devices. That is, the devices are tested and benchmarked under varying voltages, current and frequency stimuli, in temperatures ranging between cryogenic levels to 300 ℃, with their behaviour being continuously monitored.
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In the Cell Culture Laboratory, human and animal cell lines are grown in a controlled environment and aseptic conditions. Cell culture is an essential tool in multiple areas of research (health, food, pharmaceutics, cosmetics, etc.) to study basic cell biology, developmental science, or the interaction of drugs or other samples with eukaryotic cells. Different experiments are performed according to the needs of each research group. The aim is often to test samples to predict biological interactions and responses through the evaluation of cell viability, proliferation, migration and invasion, adhesion, apoptosis, oxidative stress, inflammation, among others.
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ChemLab is dedicated for air- and moisture sensitive organic synthesis, preparation and testing of covalent organic frameworks and advanced adsorbent materials and is equipped with two specialized fume hoods for materials synthesis, rotary evaporator, and a microemulsion system.
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CatLab is dedicated to testing advanced catalytic materials and characterization of materials. Catalytic setup: Fixed-bed gas-phase reactor for semihydrogenation of acetylene; high-pressure liquid-phase autoclave reactor employed for CO2 activation; proton-exchange membrane fuel cell with membrane electrode assembly for water electrolysis. Characterization equipment: TGA-DSC-MS, N2 physisorption, DLS, UV-Vis, OM, etc.; high-temperature tube furnace with controlled atmosphere.
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The optical spectroscopy part of the INL Nanophotonics & Bioimaging (NBI) open access user facility includes materials, particles, molecules and cell analysis, as well as Fourier transformed infrared spectroscopy (ATR-FTIR), Spectroscopic ellipsometer, Circular Dichroism Measurement System, Spectrophotometer UV/VIS/NIR, Fluorometer, Gel Imaging System. The open access user facility provides support in training, service measurements on spectroscopy and imaging equipment’s, as well as complementary services, such as specimen/sample preparation, spectral or image analysis.
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The optical spectroscopy part of the INL Nanophotonics & Bioimaging (NBI) open access user facility includes materials, particles, molecules and cell analysis, as well as Fourier transformed infrared spectroscopy (ATR-FTIR), Spectroscopic ellipsometer, Circular Dichroism Measurement System, Spectrophotometer UV/VIS/NIR, Fluorometer, Gel Imaging System. The open access user facility provides support in training, service measurements on spectroscopy and imaging equipment’s, as well as complementary services, such as specimen/sample preparation, spectral or image analysis.
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ChemLab is dedicated for air- and moisture sensitive organic synthesis, preparation and testing of covalent organic frameworks and advanced adsorbent materials and is equipped with two specialized fume hoods for materials synthesis, rotary evaporator, and a microemulsion system.
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Optical Lithography with positive and negative-tone resists.
Direct Laser Writing, Mask Aligner exposure for 150mm wafers, Nano-imprint.
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Mask Aligner exposure for 200mm wafers. Scanning Electron Microscppy for in-line Process Metrology and Characterization. E-beam Lithography with resolution down to 7 nm.
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Wetbenches for cleaning and wet etching processes using various chemistries. Cu eletroplating, Manual Coater for Polyimide and SU-8 Coating and Ovens
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Deep Silicon Etch for structuring and Micromachining processes, Broad-beam Ion Milling system, Deposition of metals and insulation thin films.
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Physical vapor deposition tool for the deposition of ultra–thin magnetic films. Confocal and co-deposition of a wide range of conductive and non-conductive material.
Isotropic etch of silicon and silicon dioxide.
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Deep Silicon Etch for structuring and Micromachining processes, Broad-beam Ion Milling system, Deposition of metals and insulation thin films.
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Chemical Mechanical Polishing and Planarization and CVD equipment for CNTs growth
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Physical vapor deposition tool for the deposition of ultra–thin magnetic films. Confocal and co-deposition of a wide range of conductive and non-conductive material.
Isotropic etch of silicon and silicon dioxide.
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PDMS Station, Microspotter, Drop Shape Analysis
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Optical Lithography with positive and negative-tone resists.
Direct Laser Writing, Mask Aligner exposure for 150mm wafers, Nano-imprint.
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Wetbenches for cleaning and wet etching processes using various chemistries. Cu eletroplating, Manual Coater for Polyimide and SU-8 Coating and Ovens
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Optical Lithography with positive and negative-tone resists.
Direct Laser Writing, Mask Aligner exposure for 150mm wafers, Nano-imprint.
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Mask Aligner exposure for 200mm wafers. Scanning Electron Microscppy for in-line Process Metrology and Characterization. E-beam Lithography with resolution down to 7 nm.
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